Entry | Substrates | m | n | R | Product | Yield (%)b |
1 | 7 + 3a | 10 | 2 | n-C4H9 | 12a | 85 (76) |
2 | 7 + 3b | 10 | 2 | n-C6H13 | 12b | 90 (83) |
3 | 7 + 3c | 10 | 2 | n-C8H17 | 12c | 90 (77) |
4 | 7 + 3d | 10 | 2 | n-C10H21 | 12d | 85 (82) |
5 | 7 + 3e | 10 | 2 | n-C12H25 | 12e | 80 (78) |
6 | 8 + 3a | 8 | 4 | n-C4H9 | 13a | 91 (80) |
7 | 8 + 3b | 8 | 4 | n-C6H13 | 13b | 95 (89) |
8 | 8 + 3c | 8 | 4 | n-C8H17 | 13c | 89 (83) |
9 | 8 + 3d | 8 | 4 | n-C10H21 | 13d | 83 (78) |
10 | 8 + 3e | 8 | 4 | n-C12H25 | 13e | 91 (74) |
11 | 9 + 3a | 6 | 6 | n-C4H9 | 14a | 70 (65) |
12 | 9 + 3b | 6 | 6 | n-C6H13 | 14b | 79 (60) |
13 | 9 + 3c | 6 | 6 | n-C8H17 | 14c | 75 (57) |
14 | 9 + 3d | 6 | 6 | n-C10H21 | 14d | 80 (49) |
15 | 9 + 3e | 6 | 6 | n-C12H25 | 14e | 72 (63) |
16 | 10 + 3a | 4 | 8 | n-C4H9 | 15a | 77 (51) |
17 | 10 + 3b | 4 | 8 | n-C6H13 | 15b | 70 (65) |
18 | 10 + 3c | 4 | 8 | n-C8H17 | 15c | 79 (71) |
19 | 10 + 3d | 4 | 8 | n-C10H21 | 15d | 88 (59) |
20 | 10 + 3e | 4 | 8 | n-C12H25 | 15e | 85 (69) |
21 | 11 + 3a | 2 | 10 | n-C4H9 | 16a | 48 (38) |
22 | 11 + 3b | 2 | 10 | n-C6H13 | 16b | 56 (47) |
23 | 11 + 3c | 2 | 10 | n-C8H17 | 16c | 58 (32)c |
24 | 11 + 3d | 2 | 10 | n-C10H21 | 16d | 54 (36) |
25 | 11 + 3e | 2 | 10 | n-C12H25 | 16e | 61 (40) |