Primary Analyst

C14:0

C16:0

C18:0

C22:6

C14:0

C16:0

C18:0

C22:6

C14:0

C16:0

C18:0

C22:6

Approx. Spiked Conc (%)

1.7

18

0.6

10

2.0

22.0

0.8

12

3.3

34

1.4

22

Replicate-1

96.0

96.0

86.6

117.1

95.4

90.6

96.6

106.6

92.8

86.0

88.7

106.2

Replicate-2

87.2

88.2

88.5

113.1

89.7

82.6

86.9

102.8

96.8

91.3

91.9

112.8

Replicate-3

92.7

100.3

95.1

113.0

100.8

96.7

99.7

117.4

100.5

94.3

93.2

113.6

Replicate-4

97.5

95.6

97.8

119.2

99.1

93.9

88.9

108.1

100.1

95.0

94.5

114.4

Replicate-5

89.1

82.3

80.7

111.8

93.9

89.9

91.0

115.5

96.8

91.5

91.8

111.3

Replicate-6

99.1

94.7

91.9

112.8

99.6

96.0

91.5

114.5

92.7

86.1

89.1

106.6

Replicate-7

94.2

93.3

100.3

117.1

87.3

83.2

94.1

108.1

91.8

86.6

83.1

103.9

Replicate-8

82.9

82.9

97.0

100.7

85.6

81.0

86.5

104.9

92.1

89.3

90.0

109.6

Replicate-9

93.5

90.0

96.5

113.8

82.0

80.9

87.6

104.2

90.8

87.1

88.0

105.1

Mean, primary analyst

92.5

91.5

92.7

113.2

92.6

88.3

91.4

109.1

94.9

89.7

90.0

109.3

Std Deviation

5.2

6.1

6.3

5.3

6.8

6.5

4.6

5.3

3.7

3.5

3.4

3.9

RSD (%)

5.6

6.7

6.8

4.7

7.3

7.3

5.0

4.9

3.9

3.9

3.8

3.6

Secondary Analyst

C14:0

C16:0

C18:0

C22:6

C14:0

C16:0

C18:0

C22:6

C14:0

C16:0

C18:0

C22:6

Spike-1

87.3

88.6

83.5

115.6

86.9

83.8

80.3

98.8

97.5

94.8

93.5

114.8

Spike-2

86.3

80.9

81.3

112.3

87.8

81.4

81.0

101.1

92.7

88.4

86.4

106.3

Spike-3

89.4

88.4

94.9

111.9

88.9

85.6

80.3

106.2

97.2

93.0

94.7

113.4

Mean, secondary analyst

87.7

86.0

86.6

113.3

87.9

83.6

80.5

102.0

95.8

92.1

91.5

111.5

RE (%) to Primary Analyst

−5.2

−6.0

−6.6

0.1

−5.1

−5.3

−11.9

−6.5

0.9

2.7

1.7

2.0