| Primary Analyst | C14:0 | C16:0 | C18:0 | C22:6 | C14:0 | C16:0 | C18:0 | C22:6 | C14:0 | C16:0 | C18:0 | C22:6 |
| Spiked Conc (%) | 3.2 | 41.3 | 1.7 | 25.7 | 3.9 | 48.0 | 2.4 | 32.4 | 4.6 | 54.6 | 3.0 | 39.1 |
| Replicate-1 | 100.8 | 99.9 | 97.5 | 100.9 | 103.7 | 102.8 | 100.1 | 106.0 | 103.6 | 101.9 | 100.1 | 107.2 |
| Replicate-2 | 101.9 | 101.4 | 98.7 | 102.6 | 104.4 | 103.7 | 100.8 | 107.3 | 100.8 | 99.3 | 97.4 | 104.1 |
| Replicate-3 | 102.0 | 101.3 | 99.1 | 102.7 | 100.7 | 99.9 | 97.7 | 103.6 | 101.9 | 100.4 | 98.2 | 104.7 |
| Replicate-4 | 105.0 | 104.5 | 101.7 | 97.7 | 102.1 | 101.2 | 98.8 | 103.7 | 100.6 | 99.1 | 96.8 | 103.9 |
| Replicate-5 | 102.2 | 101.8 | 99.4 | 103.2 | 101.2 | 100.4 | 98.9 | 103.8 | 101.6 | 100.2 | 97.8 | 103.9 |
| Replicate-6 | 103.6 | 103.0 | 100.6 | 104.1 | 104.0 | 103.1 | 100.5 | 106.2 | 100.5 | 99.1 | 96.8 | 103.1 |
| Replicate-7 | 101.1 | 101.4 | 99.2 | 103.3 | 102.5 | 102.0 | 99.8 | 103.8 | 101.3 | 101.3 | 99.0 | 104.3 |
| Replicate-8 | 99.5 | 100.0 | 98.7 | 101.1 | 96.2 | 97.2 | 91.6 | 96.8 | 101.0 | 100.3 | 97.5 | 102.4 |
| Replicate-9 | 100.4 | 100.7 | 98.5 | 101.7 | 101.1 | 100.4 | 99.9 | 104.9 | 103.1 | 103.5 | 101.4 | 106.8 |
| Mean, primary analyst | 101.8 | 101.6 | 99.3 | 101.9 | 101.8 | 101.2 | 98.7 | 104.0 | 101.6 | 100.6 | 98.3 | 104.5 |
| Std Deviation | 1.7 | 1.4 | 1.2 | 1.9 | 2.5 | 2.0 | 2.8 | 3.0 | 1.1 | 1.5 | 1.6 | 1.6 |
| RSD (%) | 1.6 | 1.4 | 1.2 | 1.9 | 2.4 | 2.0 | 2.9 | 2.9 | 1.1 | 1.4 | 1.6 | 1.5 |
| Secondary Analyst | C14:0 | C16:0 | C18:0 | C22:6 | C14:0 | C16:0 | C18:0 | C22:6 | C14:0 | C16:0 | C18:0 | C22:6 |
| Replicate-1 | 99.3 | 97.7 | 95.4 | 97.4 | 101.4 | 99.7 | 98.3 | 101.7 | 101.7 | 99.8 | 97.9 | 101.6 |
| Replicate-2 | 100.5 | 99.3 | 97.3 | 99.2 | 101.5 | 100.1 | 98.1 | 101.5 | 101.6 | 100.0 | 97.6 | 102.2 |
| Replicate-3 | 98.0 | 96.7 | 96.0 | 97.4 | 100.2 | 98.9 | 96.7 | 100.1 | 100.7 | 99.1 | 97.2 | 101.1 |
| Mean, secondary analyst | 99.2 | 97.9 | 96.2 | 98.0 | 101.0 | 99.6 | 97.7 | 101.1 | 101.3 | 99.6 | 97.6 | 101.6 |
| RE (%) to Primary Analyst | −2.5 | −3.6 | −3.0 | −3.9 | −0.7 | −1.6 | −1.0 | −2.8 | −0.3 | −1.0 | −0.8 | −2.7 |