A/A

RETENTION TIMES

RI

COMPONENTS

COMPOSITION (%)

GC-MS

DHS-GC-MS

A.

MeOH

Extract

B. WPES

C. Volatiles

Fraction

1.

6.00

6.31

928

α-Thujene

0.90

-

5.24

2.

6.24

6.55

937

α-Pinene

0.95

-

5.25

3.

6.78

7.07

955

Camphene

1.22

-

5.47

4.

-

7.73

977

Sabinene

-

-

0.11

5.

-

7.92

984

β-Pinene

-

-

1.19

6.

7.69

-

986

1-Octen-3-ol

1.42

0.75

-

7.

7.90

8.16

993

α-Myrcene

1.12

-

7.26

8.

8.23

-

1004

3-Octanol

0.07

-

-

9.

8.59

8.87

1013 & 1014

α-Phellandrene + δ 3-Carene

0.15

-

1.19

10.

8.95

9.21

1023

α-Terpinene

0.50

-

-

11.

9.29

9.57 *

1033

p-Cymene

21.98

0.88

39.65^*

12.

9.40

1035

Limonene

0.43

-

-

13.

9.55

9.80

1039

1,8-Cineole

1.03

-

5.23

14.

9.95

-

1049

cis-Ocimene

0.02

-

-

15.

10.49

10.75

1065

γ-Terpinene

7.79

0.23

22.02

16.

11.03

11.41

1080

trans Sabinene hydrate

1.11

0.54

0.03

17.

11.55

11.81

1093

Terpinolene

0.04

-

0.05

18.

12.14

12.47

1107

Linalool

0.87

0.55

0.09

19.

14.04

-

1153

trans-Pinocarveol

0.03

-

-

20.

14.23

-

1157

cis-Verbenol

0.04

-

-

21.

14.40

-

1161

Camphor

0.05

-

-

22.

15.40

-

1185

Borneol

3.8

4.87

-

23.

15.71

-

1192

Terpinene-4-ol

0.32

0.6

-

24.

16.11

-

1201

p-Cymen-8-ol

0.09

0.47

-

25.

16.40

-

1207

α-Terpineol

0.10

0.45

-

26.

16.60

-

1211

Dihydrocarvone

0.05

-

-

27.

18.24

18.48

1242

Thymol methyl ether

1.33

-

2.17

28.

19.21

-

1261

Thymoquinone

2.93

4.86

-

29.

21.58

-

1304

Thymol

2.01

1.82

-

30.

22.20

-

1313

Carvacrol

43.2

83.99

-

31.

31.15

-

1424

Caryophyllene

3.75

-

-

32.

32.49

-

1444

Aromadendrene

0.22

-

-

33.

33.63

-

1461

α-Humulene

0.15

-

-

34.

33.91

-

1465

Alloaromadendrene

0.04

-

-

35.

35.27

-

1480

γ-Muurolene

0.05

-

-

36.

35.85

-

1494

Viridiflorene

0.05

-

-