N˚

Atome

¹³C

(δ, ppm)

¹H

(δ, ppm) m (J, Hz)

COSY

HMBC

1

141.2

-

2

128.4

7.24 m

C-2/C-6, C-4

3

128.4

7.29 m

C-1, C-3/C-5

4

126.0

7.22 m

5

128.4

7.29 m

C-1, C-3/C-5

6

128.4

7.24 m

C-2/C-6, C-4

7

31.1

3.01 t (7.8)

H-8

C-1, C-2/C-6, C-8

8

43.9

3.42 t (7.8)

H-7

C-1, C-7, C-9

9

179.0

-

1'

109.0

-

2'

161.3

-

3'

111.9

-

4'

158.7

-

5'

113.6

-

6'

159.1

-

7'

23.6

3.88 s

C-4', C-5', C-6', C-1'', C-2'', C-6''

8'

23.0

3.95 s

C-2', C-3', C-4', C-1''', C-2''', C-6'''

1''

126.2

-

2''

152.6

-

3''

115.7

6.84 dd (1.1; 8.0)

H-4''

C-1'', C5''

4''

128.0

7.10 ddd (1.6; 8.0; 8.6)

H-3'', H-5''

C2'', C6''

5''

121.1

6.90 m

H-4'', H-6''

C1'', C3''

6''

131.6

7.44 dd (1.6; 7.6)

H-5''

C1'', C2'', C4''

1'''

126.3

-

2'''

152.6

-

3'''

115.6

6.84 dd (1.1; 8.0)

H-4'''

C-1''', C5'''

4'''

127.8

7.10 ddd (1.6; 8.0; 8.6)

H-3''', H-5'''

C2''', C6'''

5'''

121.2

6.90 m

H-4''', H-6'''

C1''', C3''

6'''

132.2

7.61 dd (1.9; 7.6)

H-5'''

C1''', C2''', C4'''

6'-OMe

63.7

3.74 s

C-6'

2'-OH

-

13.57 s

C-1', C-2', C-3'