| Continuous phase |
|
| Distilled water | 250 cc |
| Stabilizer (PVA) | CPVA = 0 - 1.0 wt%-H2O |
| Dispersed phase |
|
| PCM | 10.0g |
| TDI | 4.0 g (0.023 mol-H2O) |
| SiC | WSiC = 0 - 10 wt%-wax |
| Additive water phase |
|
| Distilled water | 30 cc |
| DETA | 2.0 g (0.019 mol-H2O) |
| Feeding velocity | 0.5 cc/min |
| Preparation of (S/O)/W dispersion |
|
| Revolution speed | Nr1 = 300 - 5000 rpm |
| Revolution time | t = 10 min |
| Temperature | T = 50˚C |
| Polymerization process |
|
| Revolution speed | Nr2 = 150 rpm |
| Revolution time | 24 h |
| Temperature | 50˚C |