Name of Chinese medicine | Names of alkaloids | Type of resin | Sample loading | Washing | Elution | Purity | Recovery | Reference | ||||
pH of the sample | Flow rate | Type | Flow rate | volume | Type and volume | Flow rate | ||||||
Corydalis yanhusuo W.T. Wang | total alkaloids | HPD-100 |
| 2 BV·h−1 | water | 3 BV·h−1 | wash to neutral | 60% ethanol 5 BV 80% ethanol 1 BV | 3 BV·h−1 |
|
| [12] |
Sophora flavescens | matrine, oxymatrine | H103 |
|
| nothing |
|
| 30% ethanol-25% ammonia water (115:1) 80% ethanol |
|
| matrine: 90.1%, oxymatrine: 85.3% | [30] |
Gelsemium elegans Benth. root | total alkaloids | AB-8 |
|
| water |
|
| 90% ethanol 4 BV | 1 - 2 mL·min−1 | 5.54% |
| [26] |
Sophora alopecuroides Linn | total alkaloids | D-101 | 9 | 5 BV·h−1 | nothing |
|
| 30% ethanol 3 BV 70% ethanol 3 BV | 1.0 BV·h−1 | 66.75% |
| [9] |
Sophora alopecuroides | total alkaloids | D-101 | 9 |
| nothing |
|
| 30% ethanol (pH = 9) 210 mL 70% ethanol (pH = 9) 210 mL |
| over 60% | >97% | [11] |
Hyoscyami Semen | total alkaloids | LSA-5B |
| 1.5 BV·h−1 | water | 1.5 BV·h−1 | 4 BV | 50% ethanol 10 BV | 1.5 BV·h−1 | 4.02% |
| [13] |
Zanthoxylum nitidum (Roxb.) DC | total alkaloids | D-101 |
| 4 BV·h−1 | nothing |
|
| The first time: 95% ethanol 4 BV | 2 BV·h−1 | 27.67% |
| [31] |
|
| nothing |
|
| The second time: 95% ethanol 3 BV | 2 BV·h−1 | ||||||
| 4 BV·h−1 | nothing |
|
| The first time: 80% ethanol 3 BV | 4 BV·h−1 | ||||||
|
| nothing |
|
| The second time: 80% ethanol 2 BV | 4 BV·h−1 | ||||||
| 4 BV·h−1 | HCl (pH = 5) |
| 1 BV | 50% ethanol 4 BV | 2 BV·h−1 | ||||||
Colchicum autumnale L. | total alkaloids | LSA-5B | 2.5 | 1.5 BV·h−1 | water |
| 8 BV | 70% ethanol 20 BV | 1.5 BV·h−1 | 12.41% | 62.27% | [10] |
Lotus leaves | total alkaloids | D-101 |
| 3 BV·h−1 | nothing |
|
| 90% ethanol 4 BV | 1.5 BV·h−1 |
| 57.2% | [32] |
Peels of Carya cathayensis Sarg. | total alkaloids | NKA-9 | 7.0 | 2 BV·h−1 | water 2 BV 30% ethanol 2 BV |
| 4 BV | 70% ethanol 4 BV | 2 BV·h−1 | 5.27% |
| [14] |
Sophora flavescens | total alkaloids | X-5 | 10 | 6 BV·h−1 | water | 2.5 BV·h−1 | 5 BV | 60% ethanol (pH = 1) | 2.5 BV·h−1 | 39.98% |
| [19] |
Lotus leaves | total alkaloids | HPD-100 | 5 - 6 | 2 mL·min−1 | water 10 BV 30% methanol 5 BV |
| 15 BV | 75% methanol 20 BV |
|
|
| [15] |
Macleaya cordata (Willd) R. Br. | rotopine alkaloids | AB-8 | 8 | 1 mL·min−1 | water |
| 1 BV | 90% ethanol 3 BV | 1 mL·min−1 | >90% |
| [33] |
Lotus leaves | total alkaloids | D-101 |
|
| water |
| 3 - 5 BV | 20% ethanol 2 BV 40% ethanol 2 BV 60% ethanol 2 BV 80% ethanol 2 BV | 1.50 BV·h−1 | 32.56% | 62.9% | [34] |