Chromatographic conditions Table

Injection mode

Splitless

Initial oven temperature

280˚C

Column

Phenomenex Zebron 5 MS

Column length

30 m

Internal diameter

0.25 mm

Film thickness

0.25 μm

Eluting gas

Helium

Elution flow rate

1 ml/min

Detection conditions

Source temperature

250˚C

Transfer line

300˚C

Electron multiplier

1660 V

Detection mode

SIM