Radiation Divergence slits Receiving slits 2θ Range (˚) | Cu, Kα1,2, I(λ1)/I(λ2) = 0.5 3.00 mm-Soller-2.00 mm -Soller-0.10 mm 8 - 160 |
Step scan Step width (2θ) Counting time (s) [range (˚2θ)] Sample | θ - θ 0.02˚ 30 [8 - 60], 40 [60 - 100], 50 [100 - 160] Powder (particle size < 90 μm) compressed in cylindrical sample holder of 24 mm diameter and 0.5 depth |
Temperature | Room temperature (293 K) |