7-OCONH2 | 156.1 C | 156.1 C | - | - |
8 | 132.7 C | 132.8 C | - | - |
8-Me | 12.7 CH3 | 12.8 CH3 | 1.80 s | 1.80 s |
9 | 133.8 CH | 133.8 CH | 5.89 m | 5.89 |
10 | 32.3 CH | 32.4 CH | 2.74 m | 2.74 m |
10-Me | 12.3 CH3 | 12.4 CH3 | 0.99 d (6.9) | 1.00 d (6.9) |
11 | 72.6 CH | 72.7 CH | 3.57 d (9) | 3.57 m |
11-OH | - | - | - | - |
12 | 81.5 CH | 81.6 CH | 3.45 m | 3.45 m |
12-OMe | 56.7 OCH3 | 56.7 OCH3 | 3.36 s | 3.36 s |
13 | 35.0 CH2 | 35.2 CH2 | 1.77 m | 1.77 m |
14 | 28.5 CH | 28.6 CH | 1.77 m | 1.77 m |
14-Me | 22.8 CH3 | 23.0 CH3 | 0.93 d (6.3) | 0.94 d (6.3) |
15a | 34.4 CH2 | 34.5 CH2 | 2.70 | 2.68 m (12.5, 9.9) |
15b | 2.40 | 2.44 m (12.5, 4.8) | ||
16 | 108.6 C | 108.5 C | - | - |
17 | 144.9 C | 145.0 C | - | - |
17-OMe | - | - | - | - |
18 | 183.8 C | 183.9 C | - | - |
19 | 108.7 CH | 108.7 CH | 7.24 s | 7.24 s |
20 | 141.4 C | 141.4 C | - | - |
21 | 180.5 C | 180.6 C | - | - |
22a | 45.7 CH2 | 45.6 CH2 | 3.91 m | 3.92 m |
22b | 3.77 m | 3.76 m | ||
23 | 25.75 CH2 | 25.8 CH2 | 3.15 t (6.6) | 3.11 t (6.6) |
24 | 111.3 C | 111.0 C | - | - |
25 | 122.5 CH | 123.4 CH | 7.13 m | 7.09 |
26 | 136.6 C | 131.8 C | - | - |
27 | 126.8 C | 127.3 C | - | - |
28 | 111.5 CH | 100.4 CH | 7.40 d (7.8) | 7.00 s |
29 | 119.8 CH | 154.3 C | 7.13 m | - |
29-OMe | - | 56.0 OCH3 | - | 3.87 s |
30 | 125.6 CH | 112.3 CH | 7.15 m | 7.29 d (9) |
31 | 118.5 CH | 112.7 CH | 7.60 d (7.8) | 6.90 d (9) |
1-NH | - | - | 9.17 s | 9.17 s |
22-NH | - | - | 6.47 brs (6.0) | 6.47 t (6.0) |
25-NH | - | - | 8.25 s | 8.14 s |