Compound (1) |
|
|
|
S2?S3 | 2.112 (3) | N1?C8 | 1.303 (11) |
S1?C8 | 1.719 (8) | N1?C9 | 1.361 (10) |
S1?C10 | 1.735 (8) | N2?C7 | 1.281 (11) |
S2?C10 | 1.742 (8) | N2?C8 | 1.394 (11) |
S3?C11 | 1.757 (7) | N3?O2 | 1.226 (11) |
S4?C11 | 1.730 (8) | N3?O3 | 1.247 (10) |
S4?C13 | 1.723 (7) | C1?O1 | 1.307 (11) |
N4?C12 | 1.390 (10) | C20?O4 | 1.336 (10) |
N4?C13 | 1.299 (11) | C9?C10 | 1.375 (11) |
N5?C13 | 1.391 (10) | C11?C12 | 1.363 (12) |
N5?C14 | 1.296 (10) | C9?C21 | 1.480 (12) |
N6?O5 | 1.240 (11) | C12?C27 | 1.481 (12) |
N6?O6 | 1.235 (11) |
|
|
C8?S1?C10 | 88.8 (4) | C8?N1?C9 | 111.0 (6) |
S3?S2?C10 | 101.4 (3) | C7?N2?C8 | 117.4 (7) |
S2?S3?C11 | 100.4 (3) | O2?N3?O3 | 122.8 (8) |
C11?S4?C13 | 88.1 (4) | C12?N4?C13 | 110.8 (6) |
O5?N6?O6 | 121.8 (8) | C13?N5?C14 | 118.7 (7) |
N4?C12?C27?C28 | 31.7 (10) | C10?C9?C21?C22 | 34.1 (12) |
C6?C7?N2?C8 | −177.1 (7) | N1?C9?C21?C26 | 31.6 (10) |
C13?N5?C14?C15 | −174.6 (7) | C11?C12?C27?C32 | 34.2 (12) |
Compound (2) |
|
|
|
Co1?O3 | 2.0124 (17) | O1?N1 | 1.230 (3) |
Co1?O4 | 2.1015 (18) | O2?N1 | 1.236 (3) |
Co1?O5 | 2.1234 (18) | O3?C1 | 1.282 (3) |
S1?O5 | 1.5263 (19) | O4?C7 | 1.235 (3) |
S1?C9 | 1.774 (3) | N1?C4 | 1.448 (3) |
S1?C8 | 1.777 (3) |
|
|
|
| O3#1?Co1?O3 | 180.0 |
O3?Co1?O5 | 90.74 (7) | O4#1?Co1?O4 | 180.0 |
O3?Co1?O4 | 88.40 (7) | O5#1?Co1?O5 | 180.0 |
O3?Co1?O4#1 | 91.60 (7) | O4?Co1?O5#1 | 94.00 (8) |
O3?Co1?O5#1 | 89.26 (7) | O4?Co1?O5 | 86.00 (8) |