| N˚ | Quantity of bleu add in mL | Duration of agitation in mn | Test + | Test − |
| 1 | 2 | 5 |
| − |
| 2 | 2 | 3 |
| − |
| 3 | 2 | 3 |
| − |
| 4 | 2 | 3 |
| − |
| 5 | 2 | 3 | + |
|
| 6 | 2 | 3 | + |
|