Run

CDPs

R_F-(VM)_n-R_F

MeOH

aq. NH₃

Yield^a)

Size of the composites^b)

(mg)

(ml)

(ml)

(ml)

(%)

(μm)

1

α-CDP (10)

300

5

1

38

5.2 ± 0.4

2

β-CDP (10)

300

5

1

56

2.8 ± 0.2

3

γ-CDP (10)

300

5

1

40

4.9 ± 0.3

4

α-CDP (25)

300

5

1

61

6.7 ± 0.4

5

β-CDP (25)

300

5

1

53

4.1 ± 0.2

6

γ-CDP (25)

300

5

1

58

6.9 ± 0.3

7

α-CDP (50)

300

5

1

62

10.9 ± 0.4

8

β-CDP (50)

300

5

1

55

4.3 ± 0.3

9

γ-CDP (50)

300

5

1

58

6.6 ± 0.4

10

α-CDP (100)

300

5

1

63

16.7 ± 0.4

11

β-CDP (100)

300

5

1

64

10.1 ± 0.3

12

γ-CDP (100)

300

5

1

61

9.6 ± 0.4

13

α-CDP (200)

300

5

1

70

10.1 ± 0.3

14

β-CDP (200)

300

5

1

66

11.2 ± 0.3

15

γ-CDP (200)

300

5

1

62

12.5 ± 0.3

16

α-CDP (300)

300

5

1

67

12.6 ± 0.3

17

β-CDP (300)

300

5

1

71

8.4 ± 0.3

18

γ-CDP (300)

300

5

1

72

11.9 ± 0.3

19

α-CDP (200)

200

5

1

78

20.5 ± 0.4

20

β-CDP (200)

200

5

1

69

7.3 ± 0.3

21

γ-CDP (200)

200

5

1

67

11.7 ± 0.5

22

α-CDP (200)

100

5

1

77

20.4 ± 0.4

Original R_F-(VM-SiO₂)_n-R_F nanoparticle

27.7 ± 6.7 nm^c)

Original α-CDP

15.8 ± 0.2 μm^b)

β-CDP

16.6 ± 0.3 μm^b)

γ-CDP

17.1 ± 0.4 μm^b)