Sample

Scaling 1

Scaling 2

Scaling 3

Volatiles

23.74 ± 0.12 w%

1.02 ± 0.07 w%

8.43 ± 0.50 w%

Ash content

61.32 ± 2.74 w%

84.29 ± 0.32 w%

68.63 ± 0.36 w%

Toluene extractable solids

25.97 ± 1.84 w%

10.21 ± 1.84 w%

34.57 ± 1.92 w%

Water and Toluene non-extractable organic Content

12.71 w%

5.5 w%

ND