Wavelength (Å) | 1.5418 |
Temperature (K) | 100 |
Detector type | MAR 345 image plate |
Detector to crystal distance (mm) | 120 |
Oscillation range per image (˚) | 0.5 |
Total rotation range (˚) | 180 |
Exposure time per frame (s) | 120 |
Space group | P21212 |
Unit-cell parameters a, b, c (Å) α, β, γ (˚) |
a = 102.6, b = 119.3, c = 66.6, α = β = γ = 90 |
Mosaicity (˚) | 0.3 |
Resolution (Å) | 40 - 1.7 (1.8 - 1.7) |
Observed reflections | 639,079 (97,092) |
Unique reflections | 85,004 (12,722) |
Redundancy | 7.5 (7.6) |
Completeness (%) | 93.9 (90.2) |
Average I/σ (I) | 30.80 (5.7) |
Rmeas (%) | 5.6 (41.4) |
CC1/2 | 1.0 (0.93) |
Overall B factor from Wilson plot (Å2) | 23.5 |