NMR data

position

1

Ref. data

δC

δH (J in Hz)

δC

δH (J in Hz)

1

158.3

158.3

2

108.3

108.3

3

174.4

174.3

4

105.5

6.55 (brs)

105.5

6.55 (d, 2.1)

5

152.1

152.2

6

105.3

6.37 (brs)

105.3

6.37 (d, 2.1)

7

190.4

190.0

8

89.5

84.0

9

138.2

138.2

10

137.1

7.11 (d, 2.0)

137.1

7.10 (d, 1.2)

11

185.7

185.7

12

104.0

5.77 (brs)

103.9

5.77 (d, 1.2)

13

169.4

169.4

14

23.2

2.44 (s)

23.2

2.44 (s)

15

56.1

3.95 (s)

56.1

3.95 (s)

16

163.5

163.5

17

56.7

3.66 (s)

56.7

3.66 (s)

18

52.8

3.69 (s)

52.8

3.69 (s)