Methods

Analyte

Extraction time (min)

Recovery

LOD (µg/L)

R²

Ref.

DLLME-GC-MS

Chlorothalonil and chlorpyrifos

2

75 - 113

0.002 - 0.5

0.998 - 0.999

[48]

IPA-LLE-HPLC-DAD

Chlorpyrifos, diazinon, fenitrothion and others

20

73 - 105

0.5 - 3.0

0.993 - 0.997

[49]

DLLME-GC-MS

Ametryn, desmetryn, dimethametryn, diprometryn, metoprotryn, prometryn and terbumetryn

-

85.2 - 114.5

0.021 - 0.12

0.978 - 0.9998

[1]

DMSPE-HRMS

Ametryn and atrazine dimethametryn

1.5

71.1 - 91.5

0.0003 - 0.006

0.9993 - 0.9999

[3]

DLLME-SFO

Diethofencarb and pyrimethanil

5

86.2 - 104.6

0.24 and 0.09

0.9995 - 0.9996

[3]

HD-DLLME-GC-MS

Atrazine, diazinon, chlorothalonil, ametryn, malathion, chlorpyrifos and dimethametryn

3

80.4 - 114.0

0.005 - 0.02

0.992 - 0.999

This study