Experiment | Reaction Temperature (˚C) z1 (x1) | [TBHP]* (mol%) z2 (x2) | [Mo]* (mol%) z3 (x3) | Reaction time (h) z4 (x4) |
1 | 60 (−1) | 50 (−1) | 0.5 (+1) | 1 (−1) |
2 | 60 (−1) | 50 (−1) | 0.1 (−1) | 5 (+1) |
3 | 60 (−1) | 70 (+1) | 0.5 (+1) | 5 (+1) |
4 | 60 (−1) | 70 (+1) | 0.1 (−1) | 1 (−1) |
5 | 80 (+1) | 50 (−1) | 0.5 (+1) | 5 (+1) |
6 | 80 (+1) | 50 (−1) | 0.1 (−1) | 1 (−1) |
7 | 80 (+1) | 70 (+1) | 0.5 (+1) | 1 (−1) |
8 | 80 (+1) | 70 (+1) | 0.1 (−1) | 5 (+1) |