Position | 1a | 1b | ||
δH | δC | δH | δC | |
1 |
| 123.5 |
| 113.5 |
2 |
| 155.3 |
| 161.0 |
3 | 7.37 (d, J = 1.5 Hz) | 111.9 | 7.09 (d, J = 1.6 Hz) | 114.0 |
4 |
| 151.6 |
| 151.9 |
5 | 7.16 (dd, J = 8.0, 1.5 Hz) | 118.3 | 7.07 (dd, J = 8.0, 1.6 Hz) | 116.7 |
6 | 7.32 (d, J = 8.0 Hz) | 129.0 | 7.77 (d, J = 8.0 Hz) | 129.7 |
7 | 5.23 (d, J = 12.4 Hz) 5.28 (d, J = 12.4 Hz) | 61.3 |
| 174.5 |
8 |
| 71.6 |
| 78.6 |
9 | 1.54 (s) | 30.4 | 1.58 (s) | 29.4 |
10 | 1.54 (s) | 30.3 | 1.68 (s) | 26.8 |
1’ | 4.93 (o) | 101.5 | 4.35 (d, J = 7.6 Hz) | 98.3 |
2’ | 3.51 | 73.5 | 3.24 | 74.0 |
3’ | 3.29 | 76.9 | 3.46 | 76.7 |
4’ | 3.42 | 70.0 | 3.30 | 70.3 |
5’ | 3.46 | 76.6 | 3.12 | 76.2 |
6’ | 3.78 (dd, 11.9, 2.4) 3.62 (dd, 11.9, 5.7) | 61.2 | 3.92 (dd, 12.1, 2.2) 3.71 (dd, 12.1, 5.6) | 61.1 |
1” |
| 171.3 |
|
|
2” | 2.70 (s) | 45.3 |
|
|
3” |
| 69.5 |
|
|
4” | 2.58 (d, J = 12.6) 2.63 (d, J = 15.6) | 45.3 |
|
|
5” |
| 175.2 |
|
|
6” | 1.38 (s) | 26.4 |
|
|