Compound

Decomp. Step

Temperature Range (˚C)

Remove Species

Wt. Loss

% (Calcd.)

% Found

[Cu₂(APA-H)(H₂O)Cl₃]·H₂O

1^st

32 - 102

−(H₂O)

3.3

3.3

2^nd

102 - 246

−(C₄H₄N₃ + Cl + H₂O)

27.2

27.1

3^rd

247 - 336

−(C₄H₃N₃)

17.2

17.1

4^th

336 - 416

−(2HCl)

13.4

14.1

5^th

417 - 569

−(N₂ + C)

7.4

7.3

residue

====

[Cu₂(O)₂] + C

31.5

31.1