Sample

Molar percent of component (%)

Total

Storage time

No.

Molar ratio

Monomeric

Dimer

Cyclic

trimer

Cyclic

tetramer

Trimer

Cyclic

octamer

Cyclic heptamer

Cyclic

decamer

Cyclic hexamer(a)

Cyclic hexamer(b)

Tetramer

(δ_(M)) (%)

Just

1

1.6

50.8

9.6

9.0

1.5

4.6

0.5

2.3

78.3

2

2.4

46.6

8.8

8.2

0.9

6.9

2.9

1.0

/

75.3

3

3.3

39.5

5.9

3.4

1.1

4.1

1.3

1.3

56.6

4

3.8

36.1

6.1

3.8

1.0

5.6

1.0

1.0

/

54.6

A month

1

1.6

43.7

10.7

9.2

2.5

7.8

2.0

0.7

/

76.6

2

2.4

38.2

8.6

8.6

0.9

7.4

0.7

3.8

68.2

3

3.3

37.8

6.0

3.7

1.1

4.4

1.3

1.3

/

55.8

4

3.8

35.3

3.2

1.7

0.6

2.0

0.7

0.7

/

44.2

Two months

1

1.6

39.5

14.4

8.0

1.3

5.1

0.5

0.5

69.3

2

2.4

37.8

8.0

2.9

1.1

7.7

1.6

1.6

64.7

3

3.3

37.4

5.1

/

/

3.2

0.8

/

3.6

0.7

1.1

51.9

4

3.8

33.2

3.7

/

/

2.3

0.8

/

2.3

0.7

0.7

43.7

Three months

1

1.6

37.0

14.2

9.2

1.3

6.4

0.8

1.0

69.9

2

2.4

36.5

8.8

8.4

2.1

7.7

2.1

2.1

67.7

3

3.3

32.3

5.3

3.6

0.6

3.8

0.8

1.0

47.4

4

3.8

30.2

5.9

3.2

1.3

3.1

2.1

2.1

47.9