Retention time/min | Components | Concentration (%) | ||||
7:00 AM | 11:00 AM | 3:00 PM | 7:00 PM | 11:00 PM | ||
1.495 | Furan, tetrahydro-3-methyl- | 2.52 | 2.22 | 2.03 | 2.04 | 1.93 |
6.9 | Bicyclo[3.1.0]hex-2-ene, 2-methyl-5-(1-methylethyl)- | 1.04 | 1.42 | 1.01 | 0.72 | 0.71 |
7.05 | alpha-pinene | 0.46 | 0.55 | 0.41 | 0.26 | 0.23 |
7.44 | camphene | 0.56 | 0.73 | 0.57 | 0.4 | 0.33 |
8.17 | beta-thujene | 4.69 | 5.47 | 3.24 | 2.31 | 2.33 |
8.25 | beta-pinene | 0.27 | 0.27 | 0.26 | 0.22 | 0.19 |
8.59 | furan, 2-pentyl- | 0.25 | 0.29 | 0.22 | 0.2 | 0.15 |
8.87 | alpha-phellandrene | 0.66 | 0.89 | 0.75 | 0.74 | 0.75 |
9.22 | (+)-2-carene | 3.97 | 3.36 | 3.27 | 3.14 | |
9.49 | benzene, 1,2,4,5-tetramethyl- | 5.82 | 7.25 | 7.09 | 5.84 | 5.62 |
9.55 | beta-phellandrene | 0.96 | 1.11 | 0.93 | 0.91 | 0.93 |
9.69 | 1,3,6-Octatriene, 3,7-dimethyl- | 0.25 | 0.33 | 0.3 | 0.24 | 0.2 |
10.19 | 1,4-Cyclohexadiene, 1-methyl-4-(1-methylethyl)- | 4.26 | 5.16 | 4.27 | 4.21 | 4.02 |
10.296 | beta-terpineol | 0.11 | ||||
10.75 | (+)-4-carene | 1.59 | 1.95 | 1.71 | 1.71 | 1.68 |
11.55 | bicyclo[3.1.0]hex-3-en-2-one, 5-(1-methylethyl)- | 9.46 | 12.02 | 12.73 | 11.8 | 11.87 |
11.854 | pinocarveol | 1.17 | ||||
12.117 | 2,6-dimethylbicyclo[3.2.1]octane | 1.37 | 1.12 | 2.12 | 1.78 | 0.9 |
12.292 | bicyclo[3.1.0]hexan-2-one, 5-(1-methylethyl)- | 2.77 | 0.19 | 1.2 | 0.94 | 1.41 |
12.836 | alpha-Thujenal | 27.81 | 26.31 | 29.47 | 28.29 | 22.16 |
13.055 | bicyclo[3.1.1]hept-2-ene-2-carboxaldehyde, 6,6-dimethyl- | 1.72 | 1.68 | 1.72 | 1.68 | 6.28 |
13.45 | Phenol, 4-(1-methylethyl)- | 1.11 | 1.18 | 1.01 | 1.09 | 0.96 |
13.755 | Propanal, 2-methyl-3-phenyl- | 5.38 | 6.86 | 6.47 | ||
14.33 | Bornyl acetate | 1.99 | 2.28 | 2.28 | 2.26 | 1.55 |
14.4 | Benzenemethanol, 4-(1-methylethyl) | 1.65 | 1.9 | 1.93 | 1.97 | 1.92 |
14.875 | o-Isopropylphenetole | 1.18 | 1.36 | 1.65 | 1.73 | 1.52 |
14.969 | g-terpinene | 1.85 | 2.17 | 2.13 | 2.35 | 2.23 |
16.896 | (+)-aromadendrene | 2.64 | 3.18 | 2.9 | 2.49 | 2.95 |
17.5 | Shyobunone | 0.5 | 0.51 | 0.99 | 0.87 | 0.95 |
18.747 | Ledol | 0.28 | 0.27 | |||
18.822 | 1,3,5,6-Tetramethyladamantane | 2 | 2.33 | 2.27 | 1.78 | 2.07 |
19.517 | 4-Isopropyl-trans-bicyclo[4.3.0]-2-nonen-8-one | 1.49 | 1.4 | 1.37 | 1.26 | 1.59 |
Total | 82.15 | 89.24 | 95.3 | 90.5 | 87.31 |