Retention time/min

Components

Concentration (%)

7:00 AM

11:00 AM

3:00 PM

7:00 PM

11:00 PM

1.495

Furan, tetrahydro-3-methyl-

2.52

2.22

2.03

2.04

1.93

6.9

Bicyclo[3.1.0]hex-2-ene, 2-methyl-5-(1-methylethyl)-

1.04

1.42

1.01

0.72

0.71

7.05

alpha-pinene

0.46

0.55

0.41

0.26

0.23

7.44

camphene

0.56

0.73

0.57

0.4

0.33

8.17

beta-thujene

4.69

5.47

3.24

2.31

2.33

8.25

beta-pinene

0.27

0.27

0.26

0.22

0.19

8.59

furan, 2-pentyl-

0.25

0.29

0.22

0.2

0.15

8.87

alpha-phellandrene

0.66

0.89

0.75

0.74

0.75

9.22

(+)-2-carene

3.97

3.36

3.27

3.14

9.49

benzene, 1,2,4,5-tetramethyl-

5.82

7.25

7.09

5.84

5.62

9.55

beta-phellandrene

0.96

1.11

0.93

0.91

0.93

9.69

1,3,6-Octatriene, 3,7-dimethyl-

0.25

0.33

0.3

0.24

0.2

10.19

1,4-Cyclohexadiene, 1-methyl-4-(1-methylethyl)-

4.26

5.16

4.27

4.21

4.02

10.296

beta-terpineol

0.11

10.75

(+)-4-carene

1.59

1.95

1.71

1.71

1.68

11.55

bicyclo[3.1.0]hex-3-en-2-one, 5-(1-methylethyl)-

9.46

12.02

12.73

11.8

11.87

11.854

pinocarveol

1.17

12.117

2,6-dimethylbicyclo[3.2.1]octane

1.37

1.12

2.12

1.78

0.9

12.292

bicyclo[3.1.0]hexan-2-one, 5-(1-methylethyl)-

2.77

0.19

1.2

0.94

1.41

12.836

alpha-Thujenal

27.81

26.31

29.47

28.29

22.16

13.055

bicyclo[3.1.1]hept-2-ene-2-carboxaldehyde, 6,6-dimethyl-

1.72

1.68

1.72

1.68

6.28

13.45

Phenol, 4-(1-methylethyl)-

1.11

1.18

1.01

1.09

0.96

13.755

Propanal, 2-methyl-3-phenyl-

5.38

6.86

6.47

14.33

Bornyl acetate

1.99

2.28

2.28

2.26

1.55

14.4

Benzenemethanol, 4-(1-methylethyl)

1.65

1.9

1.93

1.97

1.92

14.875

o-Isopropylphenetole

1.18

1.36

1.65

1.73

1.52

14.969

g-terpinene

1.85

2.17

2.13

2.35

2.23

16.896

(+)-aromadendrene

2.64

3.18

2.9

2.49

2.95

17.5

Shyobunone

0.5

0.51

0.99

0.87

0.95

18.747

Ledol

0.28

0.27

18.822

1,3,5,6-Tetramethyladamantane

2

2.33

2.27

1.78

2.07

19.517

4-Isopropyl-trans-bicyclo[4.3.0]-2-nonen-8-one

1.49

1.4

1.37

1.26

1.59

Total

82.15

89.24

95.3

90.5

87.31