Diffraction source

BL44XU, SPring-8

Wavelength (Å)

0.9

Temperature (K)

100

Detector

MX300HE

Crystal-detector distance (mm)

190

Rotation range per image (˚)

1

Total rotation range (˚)

200

Exposure time per image (s)

1

Space group

C2

a, b, c (Å)

127.2, 42.1, 63.2

α, β, γ (˚)

90.0, 114.7, 90.0

Mosaicity (˚)

0.33

Resolution range (Å)

50 - 1.37 (1.39 - 1.37)

Total No. of reflections

250,545

No. of unique reflections

62,727

Completeness (%)

98.3 (99.7)

Redundancy

4.0 (4.0)

〈I/σ(I)〉

25.3 (10.1)

Rr.i.m.

0.058 (0.194)

Overall B factor from Wilson plot (Å2)

15.2