Entry

Temp. (˚C)

MMA:Initiator

Grafting Yield

(%)

Homopolymer

Yield (%)

Grafting Efficiency (%)

Mw (×10⁶)

PDI

1

23

50:1

1.1

61

0.06

1.3

2.3

2

40

50:1

0.63

51

0.63

1.0

1.9

3

50

50:1

16

88

0.98

1.0

2.6

4

60

50:1

7.3

68

1.2

1.5

2.0

5

70

50:1

2.0

89

0.086

1.3

2.1

6

50

100:1

13

64

1.4

2.5

2.6

7

50

150:1

11

52

1.7

2.1

2.6

8

50

200:1

9.6

63

1.0

2.7

2.9

9

50

250:1

9.6

26

2.2

2.0

2.6