| synthesis from gel-like aqueous solution to melt flow (SM)1) | ||||||
| exp. No. | educts | temperature of melt step (˚C)2) | product according XRD3) | SOD-cell Parameter a0 (Å) | ||
| Zeolite 13-X | NaOH (mg) | |||||
| hydrated (mg) | dehy-drated (mg) | |||||
| SM1 | - | 200 | 50 | 330 | 13-X + amorphous | - |
| SM2 | 200 | - | - | 330 | 13-X + (NaBH4 Sod) + amorphous | - |
| SM3 | 200 | - | 50 | 330 | NaBH4 Sod + 11% amorphous | 8.935 (6) |
| SM4 | 200 | - | 50 | 350 | NaBH4 Sod | 8.9212 (6) |
| SM5 | 200 | - | 50 | 370 | NaBH4 Sod | 8.9229 (7) |