Primary Analyst

Recovery (%)

Spiked 0.1%

Spiked 0.25%

Spiked 0.4%

C14:0

C17:0

C18:0

C22:6

C14:0

C17:0

C18:0

C22:6

C14:0

C17:0

C18:0

C22:6

Day 1-1

109

108

110

105

107

108

110

106

107

106

108

105

Day 1-2

106

104

102

100

104

104

102

102

107

106

106

104

Day 1-3

109

110

110

108

108

107

105

104

106

105

105

103

Day 2-1

107

106

107

105

107

107

107

106

105

103

99

101

Day 2-2

109

109

110

108

109

110

110

109

108

106

103

104

Day 2-3

107

108

110

107

107

105

99

102

109

108

104

105

Day 3-1

100

102

109

100

107

108

106

102

108

108

101

102

Day 3-2

107

108

109

108

105

105

95

99

108

107

106

104

Day 3-3

99

100

107

98

105

105

95

99

106

106

107

103

Mean

106

106

108

104

107

106

103

103

107

106

104

104

SD

3.8

3.3

2.8

3.9

1.7

1.8

5.7

3.2

1.3

1.3

2.9

1.4

RSD (%)

3.6

3.1

2.6

3.8

1.6

1.7

5.6

3.1

1.2

1.2

2.8

1.3

Secondary Analyst

C14:0

C17:0

C18:0

C22:6

C14:0

C17:0

C18:0

C22:6

C14:0

C17:0

C18:0

C22:6

Day 1-1

107

107

98

103

106

106

100

100

108

107

99

102

Day 1-2

99

100

100

95

104

103

91

97

107

108

105

104

Day 1-3

99

100

101

96

106

107

100

102

106

107

107

103

Mean

101

102

100

98

105

105

97

100

107

107

104

103

SD

4.6

4.1

1.8

4.6

1.1

2.1

5.7

2.8

0.9

0.5

4.1

1.1

RSD (%)

4.6

4.0

1.8

4.7

1.1

2

5.8

2.8

0.8

0.5

3.9

1.1

Relative

Difference (%) to Primary Analyst

−4.2

−3.4

−8.1

−6

−1.6

−1

−6

−3.3

−0.1

0.8

−0.6

−0.6