Bruker APEX diffractometer

3009 Independent reflections

Radiation source: graphite monochromated Cu-K_α radiation

3009 reflections with I > 2 sigma(I)

R(int) = 0.0497

Absorption correction: Semi-empirical from equivalents

θ_max = 72.11˚, θ_min = 3.20˚

T_min =0.584652, T_max =0.7939

h= −12 → 10

4709 measured reflections

k = −9 → 8

l = −17 → 17