Sample | Sb(III) Added (µg∙L−1) | Propose Methodology | ETTAS | RE%* | |
Sb(III) Found ± SD (µg∙L−1) | Recovery (%, n = 4) | Sb(III) Found ± SD (µg∙L−1) | |||
1 | - | 2.04 ± 0.01 | - | 2.15 ± 0.001 | 5.11 |
0.60 | 2.632 ± 0.03 | 99.61 | |||
0.72 | 2.748 ± 0.05 | 99.41 | |||
2 | - | 1.39 ± 0.06 | - | 1.30 ± 0.02 | 6.47 |
0.60 | 1.987 ± 0.02 | 100.52 | |||
0.72 | 2.105 ± 0.08 | 101.43 | |||
3 | - | 1.98 ± 0.03 | - | 1.84 ± 0.003 | 7.07 |
0.60 | 2.587 ± 0.06 | 99.78 | |||
0.72 | 2.703 ± 0.06 | 100.15 | |||
4 | - | 2.22 ± 0.06 | - | 2.50 ± 0.04 | 11.2 |
0.60 | 2.830 ± 0.02 | 100.45 | |||
0.72 | 2.943 ± 0.07 | 100.13 | |||
5 | - | 0.33 ± 0.03 | - | 0.303 ± 0.07 | 8.18 |
0.36 | 0.679 ± 0.01 | 96.66 | |||
0.48 | 0.803 ± 0.04 | 97.87 | |||
6 | - | 0.16 ± 0.04 | - | | - |
0.36 | 0.523 ± 0.02 | 101.87 | |||
0.48 | 0.644 ± 0.05 | 102.50 | |||
7 | - | 1.06 ± 0.02 | - | 1.10 ± 0.02 | 3.63 |
0.36 | 1.411 ± 0.05 | 99.15 | |||
0.48 | 1.537 ± 0.01 | 99.72 | |||
8 | - | 1.45 ± 0.04 | - | - | - |
0.36 | 1.804 ± 0.07 | 99.59 | |||
0.48 | 1.919 ± 0.07 | 99.24 | |||
9 | - | 3.23 ± 0.03 | - | 3.15 ± 0.07 | 1.54 |
0.60 | 3.841 ± 0.02 | 100.34 | |||
0.72 | 3.955 ± 0.09 | 100.15 | |||
10 | - | 2.91 ± 0.01 | - | 3.02 ± 0.01 | 3.64 |
0.60 | 3.501 ± 0.02 | 99.69 | |||
0.72 | 3.647 ± 0.03 | 100.58 |