Spectral lines | Mo | Fe | ||
Sample preparation | Pressed pellet | Borate fusion | Pressed pellet | Borate fusion |
Spectral line | Mo LA1-HR-Min (High resolution line) | Fe KA1-Maj (Majority line) | ||
Mode | Atmospheric He | Vacuum | Atmospheric He | Vacuum |
Tube voltage (kV) | 27 | 30 | 50 | 50 |
Tube current (mA) | 112 | 77 | 10 | 8 |
Crystal (2d, Å) | PET (8.752) | LiF200 (4.026) | ||
Collimator aperture (degree) | 0.23 | 0.23 | ||
Detector | Flow | Scintillation | ||
Adjusted peak (2q) | 76.360 | 76.327 | 57.527 | 57.537 |
Wavelength (Å) | 5.405 | 1.936 | ||
Position of background (2q) | 77.612 | 74.542 | 58.470 | 58.346 |