Yield Size of nanocompositesa)

Run Oligomer h-BN aq. NH3 Product Before calcination After calcination

(mg) (mg) (ml) (mg) (nm) ± STD (nm) ± STD

RF-(ACA)n-RF

1 20 100 5 92 (77)b)[11]c) 55.8 ± 15.2 37.3 ± 10.3

2 50 100 5 119 (79)b)[6]c) 38.4 ± 7.6 80.6 ± 19.3

3 100 100 5 128 (64)b)[14]c) 128.5 ± 26.6 25.5 ± 5.3

4 200 100 5 228 (76)b)[18]c) 35.6 ± 8.2 53.2 ± 11.8

5 20 100 0 88 (73)b)[24]c) 17.0 ± 3.5 18.3 ± 4.7

6 50 100 0 93 (62)b)[50]c) 53.7 ± 10.0 44.8 ± 9.1

7 100 100 0 88 (44)b)[76]c) 46.5 ± 8.9 19.6 ± 5.0

8 200 100 0 90 (30)b)[186]c) 48.4 ± 10.0 28.6 ± 2.9

RF-(DMAA)n-RF

9 50 100 5 80 (53)b)[53]c) 29.4 ± 8.3 90.1 ± 13.7

10 100 100 5 68 (34)b)[81]c) 44.0 ± 5.8 59.6 ± 9.5

11 150 100 5 80 (32)b)[135]c) 95.2 ± 24.4 105.5 ± 19.4

12 200 100 5 84 (28)b)[180]c) 166.7 ± 37.6 131.7 ± 25.6

13 50 100 0 93 (62)b)[39]c) 44.1 ± 9.5 63.4 ± 10.4

14 100 100 0 92 (46)b)[79]c) 39.0 ± 10.5 160.9 ± 30.4

15 150 100 0 93 (37)b)[123]c) 70.8 ± 13.5 174.2 ± 40.0

16 200 100 0 93 (31)b)[150]c) 85.2 ± 17.0 113.2 ± 25.3