1

2

3

δH m (J in Hz)

δc

δH m (J in Hz)

δc

δH m (J in Hz)

δc

1

-

33.9

-

36.9

-

37.2

2a

2b

1.41 dd (14.52; 3.03)

1.74 dd (14.52; 3.13)

46.1

1.52 dd (14.60; 3.03)

1.89 dd (14.60; 3.13)

40.6

1.40 d (14.76)

1.81 dd (14.76; 3.16)

41.4

3

3.91 m

71.3

3.95 m

71.3

4.03 m

66.7

4

3.06 dd (10.59; 3.23)

78.2

3.06 dd (10.59; 3.23)

78.2

1.70 t (13.12), 1.53 d (13.89)

35.8

5

1.80 m

33.8

2.12 m

33.8

2.28 m

29.6

6

1.48 t (10.03)

58.1

-

79.7

-

78.1

7

5.47 dd (15.43; 9.65)

133.7

5.75 dd (15.43; 9.65)

135.2

5.78 d (15.12)

135.1

8

5.38 dd (15.43; 6.43)

133.2

5.66 dd (15.43; 6.43)

128.6

5.69 dd (15.12; 5.04)

128.7

9

4.11 m

74.4

4.21 m

74.4

4.21 m

72.9

10

3.46 dd (16.33; 4.50)

67.6

3.50 dd (11.96; 4.50)

67.6

3.46 ddd (11.96; 4.50)

66.3

11

0.79 s

32.4

0.81 s

24.9

0.82 s

26.3

12

1.02 s

24.1

1.15 s

26.3

1.158 s

24.9

13

0.94 d (6.45)

17.2

0.98 d (6.45)

10.6

0.84 d (6.48)

15.0