Molar ratio of initial reagents | Temperature of reaction mixture, К | Viscosity, mm2/s | Content of FAEE, % in the samples by viscosity correlation (2) | Content of FAEE, % in the samples according to the data of GC-MS |
6:1 | 623 | 14.466 | 41.58 | 42.41 |
638 | 14.412 | 41.76 | 49.87 | |
653 | 12.444 | 49.01 | 50.26 | |
8:1 | 623 | 9.444 | 62.64 | 63.21 |
638 | 8.844 | 65.88 | 65.12 | |
653 | 6.828 | 78.66 | 80.11 | |
10:1 | 638 | 8.394 | 68.46 | 68.34 |
653 | 6.636 | 80.07 | 80.54 | |
12:1 | 608 | 9.882 | 60.40 | 60.39 |
623 | 8.802 | 66.12 | 66.50 | |
638 | 7.578 | 73.51 | 72.77 | |
653 | 6.036 | 84.75 | 81.92 | |
16:1 | 653 | 4.986 | 94.19 | 92.08 |
18:1 | 623 | 5.302 | 91.15 | 92.25 |
638 | 5.040 | 93.65 | 93.66 | |
653 | 4.830 | 95.76 | 94.56 | |
20:1 | 608 | 8.002 | 70.82 | 71.12 |
623 | 6.054 | 84.60 | 85.41 |