Material | Primary components | pH | Mode of application |
Clearfil SE Bond adhesive system (Kuraray Noritake Dental; Sakazu, Kurashiki, Okayama, Japan) Batch No. Primer: 9N0168 Adhesive: 9U0269 | Primer: 10-MDP, HEMA, hydrophilic methacrylate, dl-camphorquinone, N,N-dihydroxyethyl-p-toluidine, water. Bond: 10-MDP, bis-GMA, HEMA, hydrophobic methacrylate, dl-camphorquinone, N,N-dihydroxyethyl-p-toluidine, silanized colloidal silica | 2.0 | 1) Active application of primer to the dry dentin surface for 20 s 2) Gentle air-jet drying for 5 s 3) Application of bonding agent 4) Gentle air-jet drying for 5 s 5) Light-curing for 10 s |
Sodium bicarbonate (Biodinâmica Química e Farmacêutica LTDA; Ibiporã, Paraná, Brazil) Batch No.: 321/15 | Sodium bicarbonate (NaHCO3) and flavouring agents | 8.0 | Dilution: 200 mg sodium bicarbonate in 10 mL normal saline 1) Active application to the dry dentin surface for 60 s 2) Removal of excess solution |
Chlorhexidine (FGM Dentscare LTDA; Joinville, Santa Catarina, Brazil) Batch No.: 050815 | 2% chlorhexidine digluconate, deionized water, volatile surfactant | 5.5 - 7 | 1) Active application to the dry dentin surface for 60 s 2) Removal of excess solution |
Filtek Z350 XT (3M ESPE; St Paul, MN, USA) Batch No.: 1535700494 | Silane-treated ceramic filler, bisphenol A-glycidyl methacrylate (bis-GMA), bisphenol A-polyethylene glycol diether dimethacrylate (bis-EMA), silane-treated silicon dioxide filler, silane-treated silica/zirconia filler, diurethane dimethacrylate, polyethylene glycol dimethacrylate, triethylene glycol dimethacrylate (TEG-DMA), 2,6-di-tert-butyl-p-cresol (BHT), pigments | _ | 1) Composite resin build-up technique 2) Light-curing for 40 s |