N˚ C | 13C(δ, ppm) | DEPT 135 | 1H*(δ, ppm) | HMBC |
1 | 110.63 | CH | 6.55 (dd, 1H, Pyrim.) | ─ |
2, 6 | 158.42 | CH | 8.23 (d, 2H, Pyrim.) | ─ |
4 | 164.10 | ─ | ─ | 2.4 |
8 | 164.10 | ─ | ─ | ─ |
9 | 154.96 | ─ | ─ | 20.9 |
10 | 136.48 | ─ | ─ | ─ |
11 12 13 14 15 | 131.07 124.63 128.70 124.63 131.07 | CH | 7.97 (m, 1H, Harom.) 8.01 (m, 1H, Harom.) 7.55 (m, 1H, Harom.) 8.01 (m, 1H, Harom.) 7.97 (m, 1H, Harom.) | ─ |
17 18 19 20 ─ | 149.05 127.22 133.47 138.47 ─ |
CH
H2O | 8.74 (d, 1H, Pyr.) 7.68 (t, 1H, Pyr.) 7.68 (td, 1H, Pyr.) 8.08 (d, 1H, Pyr.) 3.36 (s, 2H2O) | ─ |