| Solvent | Amount taken μg·mL−1 | Amount found μg·mL−1 | Rec.% |
| SD | RSD |
|
| Confidence limits |
Complex (DAT:CLA) | Ethanol | 9.91 | 9.87 | 99.60 | 100.33 | 0.7572 | 0.7547 | 0.33 | ±0.9401 | 100.33 ± 0.9401 |
15.85 | 15.80 | 99.68 | ||||||||
19.82 | 20.10 | 101.41 | ||||||||
27.75 | 28.00 | 100.90 | ||||||||
35.67 | 35.70 | 100.08 | ||||||||
Methanol | 11.90 | 11.90 | 100.00 | 99.87 | 0.8312 | 0.8323 | 0.13 | ±1.0320 | 99.87 ± 1.0320 | |
17.84 | 17.80 | 99.78 | ||||||||
25.76 | 25.62 | 99.46 | ||||||||
33.69 | 33.60 | 99.73 | ||||||||
39.64 | 39.80 | 100.40 | ||||||||
Complex (MTDA:CLA) | Ethanol | 10.01 | 10.4 | 104.00 | 101.0 | 1.956 | 1.94 | 0.10 | ±2.428 | 101.0 ± 2.428 |
17.52 | 17.6 | 100.00 | ||||||||
25.03 | 25.0 | 100.00 | ||||||||
32.53 | 32.2 | 99.00 | ||||||||
45.05 | 44.9 | 99.60 | ||||||||
Methanol | 7.50 | 7.76 | 103.0 | 101.0 | 1.505 | 1.49 | 0.10 | ±1.868 | 101.0 ± 1.868 | |
17.52 | 17.50 | 99.8 | ||||||||
25.03 | 25.4 | 101.0 | ||||||||
30.03 | 29.9 | 99.6 | ||||||||
35.04 | 35.4 | 101.0 |