Entry
Starting Material
Product
Temp. (oC)
Time (h)
Yielda (%)
1
reflux
8
quant
2
reflux
2
77
3
reflux
2
quant
4
50
6
69
5
reflux
2
71
6
reflux
6
77
7
reflux
16
84
8
reflux
2
83
9
reflux
6
56
| Entry | Starting Material | Product | Temp. (oC) | Time (h) | Yielda (%) |
| 1 |
|
| reflux | 8 | quant |
| 2 |
|
| reflux | 2 | 77 |
| 3 |
|
| reflux | 2 | quant |
| 4 |
|
| 50 | 6 | 69 |
| 5 |
|
| reflux | 2 | 71 |
| 6 |
|
| reflux | 6 | 77 |
| 7 |
|
| reflux | 16 | 84 |
| 8 |
|
| reflux | 2 | 83 |
| 9 |
|
| reflux | 6 | 56 |