Entry
Starting Material
Product
Temp. (˚C)
Time (h)
Yielda (%)
1
50
22
13
2
reflux
6
23
3
dec
reflux
1
NA
4
dec
reflux
2
NA
5
NR
reflux
2
NA
| Entry | Starting Material | Product | Temp. (˚C) | Time (h) | Yielda (%) |
| 1 |
|
| 50 | 22 | 13 |
| 2 |
|
| reflux | 6 | 23 |
| 3 |
| dec | reflux | 1 | NA |
| 4 |
| dec | reflux | 2 | NA |
| 5 |
| NR | reflux | 2 | NA |