N˚ | Temperature | Time | ∆m [%] | N˚ | Temperature | Time | ∆m [%] |
1 | 370˚C | 1 hour | 21.00 | 7 | 420˚C | 3 hours | 28.00 |
2 | 370˚C | 2 hours | 26.60 | 8 | 420˚C | 4 hours | 33.50 |
3 | 370˚C | 3 hours | 22.50 | 9 | 470˚C | 1 hour | 34.40 |
4 | 370˚C | 4 hours | 25.50 | 10 | 470˚C | 2 hours | 37.80 |
5 | 420˚C | 1 hour | 31.80 | 11 | 470˚C | 3 hours | 38.00 |
6 | 420˚C | 2 hours | 33.43 | 12 | 470˚C | 4 hours | 43.50 |