Sample

time

650˚C

700˚C

750˚C

800˚C

α

EB

α

EB

α

EB

α

EB

#O2

2 h

6.8

24.7

7.0

21.3

7.3

23.5

7.0

23.3

#N2

2 h

6.5

23.1

6.5

23.2

7.5

23.2

7.1

21.6

#O2.5

2.5 h

6.5

22.4

7.3

22.6

8.1

22.7

7.5

20.5

#N2.5

2.5 h

6.9

21.3

7.2

21.5

8.0

23.0

7.5

19.8

#O3

3 h

7.1

23.2

7.7

23.5

8.9

19.1

8.0

23.1

#N3

3 h

6.8

22.7

7.5

23.3

8.4

20.6

7.9

21.7

#O3.5

3.5 h

7.2

21.7

7.7

21.8

7.9

21.2

7.2

21.3

#N3.5

3.5 h

7.1

22.0

7.4

20.2

7.8

22.4

7.4

23.4

#O4

4 h

6.7

23.3

7.0

22.5

7.4

22.0

7.2

22.8

#N4

4 h

6.8

21.8

7.3

22.8

7.2

22.4

6.9

21.9