Entry

Condition^a

Reaction time (s)

Temperature

(˚C)

H₂NOH

(mmol)

Conversion

(%)^b

1

Irradiation of MW (100 W)

240

68

0.35

45

syn:anti = 20:80

2

Irradiation of MW (100 W)

240

68

0.70

65

syn:anti = 23:77

3

Irradiation of MW (100 W)

240

68

1.40

97

syn:anti = 11:89

4

Irradiation of MW (300 W)

120

113

0.70

61

syn:anti = 20:80

5

Conventional heating

240

68

0.35

38

syn:anti = 16:84

6

Conventional heating

240

68

0.70

74

syn:anti = 22:78

7

Conventional heating

240

68

1.40

97

syn:anti = 9:191

8

Conventional heating

120

113

0.70

58

syn:anti = 14:86