Entry

Condition^a

Reaction time (s)

Temperature

(˚C)

H₂NOH

(mmol)

Conversion

(%)^b

1

Irradiation of MW (100 W)

240

68

0.35

16

syn:anti = 0:100

2

Irradiation of MW (100 W)

240

68

0.70

19

syn:anti = 11:89

3

Irradiation of MW (100 W)

240

68

1.40

55

syn:anti = 13:87

4

Irradiation of MW (300 W)

120

113

0.70

92

syn:anti = 5:95

5

Conventional heating

240

68

0.35

14

syn:anti = 0:100

6

Conventional heating

240

68

0.70

34

syn:anti = 21:79

7

Conventional heating

240

68

1.40

51

syn:anti = 8:92

8

Conventional heating

120

113

0.70

91

syn:anti = 10:90