| Run order | A-acetone conc. %(v/v) | B-Temp ˚C | C-Solid/Solvent ratio. % (w/v) | D-Time, min |
| 1 | 40.0 | 60.0 | 1.0 | 90.0 |
| 2 | 60.0 | 35.0 | 1.0 | 60.0 |
| 3 | 40.0 | 10.0 | 8.0 | 90.0 |
| 4 | 40.0 | 10.0 | 1.0 | 90.0 |
| 5 | 60.0 | 35.0 | 4.5 | 60.0 |
| 6 | 40.0 | 60.0 | 8.0 | 30.0 |
| 7 | 100.0 | 35.0 | 4.5 | 60.0 |
| 8 | 40.0 | 10.0 | 8.0 | 30.0 |
| 9 | 60.0 | 35.0 | 4.5 | 60.0 |
| 10 | 20.0 | 35.0 | 4.5 | 60.0 |
| 11 | 40.0 | 10.0 | 1.0 | 30.0 |
| 12 | 40.0 | 60.0 | 8.0 | 90.0 |
| 13 | 60.0 | 10.0 | 4.5 | 60.0 |
| 14 | 60.0 | 35.0 | 11.5 | 60.0 |
| 15 | 80.0 | 60.0 | 8.0 | 90.0 |
| 16 | 60.0 | 35.0 | 4.5 | 5.0 |
| 17 | 80.0 | 10.0 | 8.0 | 30.0 |
| 18 | 60.0 | 35.0 | 4.5 | 60.0 |
| 19 | 80.0 | 10.0 | 8.0 | 90.0 |
| 20 | 80.0 | 60.0 | 1.0 | 30.0 |
| 21 | 60.0 | 35.0 | 4.5 | 120.0 |
| 22 | 80.0 | 60.0 | 1.0 | 90.0 |
| 23 | 80.0 | 60.0 | 8.0 | 30.0 |
| 24 | 60.0 | 35.0 | 4.5 | 60.0 |
| 25 | 60.0 | 35.0 | 4.5 | 60.0 |
| 26 | 60.0 | 85.0 | 4.5 | 60.0 |
| 27 | 80.0 | 10.0 | 1.0 | 90.0 |
| 28 | 80.0 | 10.0 | 1.0 | 30.0 |
| 29 | 40.0 | 60.0 | 1.0 | 30.0 |
| 30 | 60.0 | 35.0 | 4.5 | 60.0 |