Chemical formula

(C₈H₉N₂)₃[Al(C₂O₄)₃]∙3H₂O

Formula weight (g∙mol⁻¹)

744.60

Temperature (K)

298

Crystal system; Space group

Monoclinic; P2₁/c

a(Å); b(Å); c(Å); β(˚)

13.499(7); 14.872(9); 16.995(5)D:\srp_word_html20170901\Word_xml\bin\Debug\docTempWords\zid5b _cell_length_c; 91.44(3)

Volume (ų); Z

3411(3); 4

Sample size (mm)

0.24 × 0.15 × 0.08

Radiation, λ, (Å)

λ = 0.71073

μ (mm⁻¹)

0.14

F₀₀₀

1552

θ Range (˚)

2.0 ≤ θ ≤ 27.2

Scan mode

ω − 2θ

Absorption correction

psi-scan

T_min, T_max

0.8948; 0.9999

Number of reflections measured;

Independent reflections; R_int,

8630

7540; 0.0603

Reflections with [I > 2σ (I)]

3695

R(F²); ωR(F²); S (GOOF)

0.0782; 0.2472; 1.016

Δρ_max, Δρ_min (e∙Å⁻³)

0.63; −0.41*