| 2 | (22E, 24R)-5α,8α-epidioxyergosta- 6,9(11),22-trien-3β-ol | |||
| atom | δC | δH (J in Hz) | δC | δH (J in Hz) |
| 1 | 32.5 |
| 32.5 |
|
| 2 | 30.6 |
| 30.5 |
|
| 3 | 66.3 | 4.01 m | 66.3 | 4.01 m |
| 4 | 36.0 |
| 36.0 |
|
| 5 | 82.7 |
| 82.7 |
|
| 6 | 135.4 | 6.29 (d, 8.3) | 135.4 | 6.27 (d, 8.4) |
| 7 | 130.7 | 6.60 (d, 8.3) | 130.7 | 6.58 (d, 8.4) |
| 8 | 78.3 |
| 78.3 |
|
| 9 | 142.5 |
| 142.4 |
|
| 10 | 37.9 |
| 37.9 |
|
| 11 | 119.7 | 5.43 (dd, 5.8, 1.5) | 11.97 | 5.41 (dd, 6.0, 0.8) |
| 12 | 41.2 |
| 41.1 |
|
| 13 | 43.6 |
| 43.6 |
|
| 14 | 48.1 |
| 48.1 |
|
| 15 | 20.9 |
| 20.8 |
|
| 16 | 28.6 |
| 28.7 |
|
| 17 | 55.8 |
| 55.8 |
|
| 18 | 12.9 | 0.74 s | 12.9 | 0.71 s |
| 19 | 25.5 | 1.09 s | 25.5 | 1.06 s |
| 20 | 39.9 |
| 39.9 |
|
| 21 | 20.7 | 1.00 (d, 6.9) | 20.7 | 0.98 (d, 6.4) |
| 22 | 135.1 | 5.17 (dd, 15.5, 8.3) | 135.1 | 5.15 (dd, 15.2, 7.2) |
| 23 | 132.4 | 5.25 (dd, 15.5, 8.3) | 132.4 | 5.27 (dd, 15.2, 8.0) |
| 24 | 42.7 |
| 42.7 |
|
| 25 | 33.0 |
| 33.0 |
|
| 26 | 19.9 | 0.84 (d, 6.9) | 19.9 | 0.81 (d, 6.8) |
| 27 | 19.6 | 0.82 (d, 6.9) | 19.6 | 0.80 (d, 6.4) |
| 28 | 17.5 | 0.92 (d, 6.9) | 17.5 | 0.89 (d, 6.8) |