| Sample | Weight (g) | Volume (L) | Dilution |
| Digested Blank #1 | 0 | 0.020 | 100.000 |
| Digested Blank #2 | 0 | 0.020 | 100.000 |
| 5% Pd BaSO4 Sample 1 | 0.211 | 0.020 | 100.000 |
| 5% Pd BaSO4 Sample 1 dup. | 0.211 | 0.020 | 100.000 |
| 5% Pd BaSO4 Sample 2 | 0.1994 | 0.020 | 100.000 |
| 5% Pd BaSO4 Sample 2 dup. | 0.1994 | 0.020 | 100.000 |
| 5% Pd BaSO4 Sample 1 Spiked | 0.1998 | 0.020 | 100.000 |
| 5% Pd BaSO4 Sample 1 Spiked dup. | 0.1998 | 0.020 | 100.000 |
| Sample | Weight (g) | Volume (L) | Dilution |
| Digested Blank #1 | 0 | 0.020 | 100.000 |
| Digested Blank #2 | 0 | 0.020 | 100.000 |
| 5% Pd BaSO4 Sample 1 | 0.211 | 0.020 | 100.000 |
| 5% Pd BaSO4 Sample 1 dup. | 0.211 | 0.020 | 100.000 |
| 5% Pd BaSO4 Sample 2 | 0.1994 | 0.020 | 100.000 |
| 5% Pd BaSO4 Sample 2 dup. | 0.1994 | 0.020 | 100.000 |
| 5% Pd BaSO4 Sample 2 Spiked | 0.1998 | 0.020 | 100.000 |
| 5% Pd BaSO4 Sample 2 Spiked dup. | 0.1998 | 0.020 | 100.000 |