Sample Introduction (AOC 20i, Shimadzu, Japan) | Mode | Splitless |
Injector Temperature | 240˚C | |
Injection Volume | 1 µL | |
Gas Chromatograph (GC 2010Plus, Shimadzu, Japan) | Capillary Column | Shimadzu InertCap Wax (30.0 m × 0.25 mm × 0.25 µm film thickness) |
Carrier Gas | Helium (99.999%) | |
Column Flow Rate | 1.53 mL・min−1 | |
Oven Temperature Program | 70˚C (held 3 min), ramped to 150˚C at 15˚C min−1 (held 2 min), and a final ramp to 240˚C at 15˚C min−1 (held 8 min) | |
Run Time | 21.33 min | |
Mass Spectrometer (QPMS 2010Ultra, Shimadzu, Japan) | Acquisition Mode | FASST |
Mass Range (m/z) | 35 - 400 amu | |
Solvent Delay | 6.4 min | |
Source Temperature | 200˚C | |
Transfer Line Temperature | 240˚C | |
Electron Energy | 70 eV |