Analytical methods

Analyte studied

Sample type and its volume (mL)

LDR (µg/L)

LODs (µg/L)

%RDS

Extraction time (min)

Ref.

SALLE-capillary LC-DAD

Cephoperazone, cefquinome, cephalexin, cephapirin, cephaloniun, cephamandole, cephazolin and cephadroxile

Water (4)

1.3 - 100

0.4 - 1.3

0.6 - 9.9

<10

[26]

SALLE-capillary LC-DAD

Cephoperazone, cefquinome, cephalexin, cephapirin, cephaloniun, cephamandole, cephazolin and cephadroxile

Banana juice (2.5)

10 - 500

3 - 13

1.2 - 9.9

<10

[26]

CPE-HPLC-DAD

Thiamethoxam, imidacloprid, acetamiprid, thiacloprid

Water (18)

4 - 2000

0.8 - 1.2

-

17

[41]

IL-MNPs based SPE-capillary LC-DAD

Thifensulfuron methyl, metsulfuron methyl, triasulfuron, tribenuron methyl and primisulfuron methyl

Water (50)

5 - 100

5 - 100

2.3 - 4.9

-

[42]

Au-TEOS based SPE-capillary LC-DAD

Bensulfuron-methyl, metsulfuron-methyl, pyrazosulfuron-methyl, thifensulfuron-methyl and triasulfuron

Water (10)

50 - 1000

2 - 9

2.1 - 4.5

-

[43]

Au-NP-IL-silica based SPE-capillary LC-DAD

Bensulfuron-methyl, metsulfuron-methyl, pyrazosulfuron-methyl, thifensulfuron-methyl and triasulfuron

Water (10)

50 - 1000

2 - 6

2.8 - 4

-

[43]

SPE-CE-UV

Triasulfuron, rimsulfuron, flazasul-furon, metsulfuron-methyl and chlorsulfuron

Aqueous extract of grapes (250)

0.97 - 200

(µg/kg)

0.97 - 8.3 (µg/kg)

5.2 - 21.4

>120

[44]

SPE-HPLC-MS

Amidosulfuron, Aimsulfuron, Nicosulfuron, Thifensulfuron Methyl, Tribenuron Methyl and Azoxystrobin

Water (1000)

15 - 150

5 - 8.1

-

> 60

[45]

SALLE-HPLC-DAD

Carbaryl, atrazine, propazine,

Lake water (5)

7 - 100

2 - 2.8

1 - 7.8

<8

Current study

chlorothalonil, dimethametryn and terbutryn

River water (5)

1.6 - 10

Ground water (5)

0.67 - 6.42