Entry

Catalyst (wt.%)

Solvent

Temp ˚C

Time (h)

Yield (%)a

1

5

Neat

RT

24

35

2

5

MeOH

RT

24

25

3

5

EtOH

RT

24

30

4

5

THF

RT

4

10

5

5

Neat

50

1.5

95

6

0

Neat

50

6.5

70

7

10

Neat

50

1.5

83

8

15

Neat

50

1.5

70

9

5

MeOH

50

4.0

75

10

5

EtOH

50

4.5

69

11

5

IPA

50

6

70