Parameter

1

Emprical formula

C₃₈H₃₄N₄O₁₄Ni

T (K)

293(2)

Wavelength (Å)

0.71069

Crystal system

Triclinic

Space group

P-1

a (Å)

18.796(5)

b (Å)

10.121(5)

c (Å)

20.513(5)

α

90.000(5) deg.

β

98.312(5) deg.

γ

90.000(5) deg.

V (ų)

3861(2)

Z

4

D_calc. (mg∙m⁻³)

1.427

Absorption coefficient (mm⁻¹)

0.576

F (000)

1720

Crystal size (mm)

0.31 × 0.26 × 0.24

θ (Range of data collection)

2.01 to 28.27 deg.

Limiting indices

−22 ≤ h ≤ 24,

−13 ≤ k ≤ 11,

−26 ≤ l ≤ 26

Data [1 > 2σ(1)]

4667/0/266

Goodnes of fit on F²

0.943

R_1, wR₂ indices (1 > 2σ(1))^a

R₁ = 0.0517, wR₂ = 0.1396

R₁, wR₂ (all data)

R₁ = 0.0747, wR₂ = 0.1544