Position | 1a* (in MeOD) | 1b* (in MeOD) | 1c** (in MeOD) | 1d** (in MeOD) | 5a* (in CDCl3-MeOD) |
1 | 34.6 | 34.6 | 34.7 | 34.6 | 16.9 |
2 | 38.2 | 38.2 | 38.2 | 38.2 | 32.6 |
3 | 219.2 | 219.3 | 219.0 | 219.1 | 75.7 |
4 | 51.1 | 51.1 | 51.1 | 51.1 | 48.5 |
5 | 49.3 | 49.3 | 49.4 | 49.4 | 37.6 |
6 | 21.9 | 21.9 | 21.9 | 21.9 | 41.8 |
7 | 27.9 | 27.9 | 28.1 | 28.1 | 18.0 |
8 | 46.8 | 46.8 | 47.0 | 46.9 | 52.3 |
9 | 21.7 | 21.7 | 21.6 | 21.6 | 38.2 |
10 | 28.5 | 28.5 | 28.5 | 28.6 | 61.7 |
11 | 29.4 | 29.4 | 29.4 | 29.4 | 39.0 |
12 | 34.9 | 34.9 | 35.0 | 35.0 | 27.7 |
13 | 48.5 | 48.5 | 48.9 | 48.9 | 52.5 |
14 | 63.8 | 63.8 | 64.4 | 64.4 | 41.5 |
15 | 32.6 | 32.6 | 32.5 | 32.4 | 28.7 |
16 | 30.4 | 30.4 | 30.6 | 30.5 | 37.0 |
17 | 53.6 | 53.6 | 54.1 | 53.8 | 31.9 |
18 | 18.4 | 18.5 | 18.3 | 18.3 | 44.1 |
19 | 30.6 | 30.6 | 30.8 | 30.8 | 27.1 |
20 | 35.8 | 35.9 | 36.6 | 36.8 | 141.9 |
21 | 18.5 | 18.6 | 18.8 | 18.8 | 74.9 |
22 | 33.0 | 33.3 | 34.3 | 34.5 | 40.1 |
23 | 26.4 | 26.6 | 28.7 | 28.5 | 11.6 |
24 | 77.8 | 80.7 | 78.6 | 90.7 | 16.1 |
25 | 84.2 | 72.8 | 73.9 | 74.4 | 20.3 |
26 | 22.7 | 25.6 | 25.8 | 25.8 | 18.3 |
27 | 22.5 | 25.9 | 24.8 | 25.7 | 179.3 |
28 | 22.6 | 22.7 | 22.6 | 22.6 | 33.9 |
29 | 21.4 | 21.4 | 21.4 | 21.4 | 117.1 |
30 | 180.1 | 180.1 | 178.4 | 178.4 |
|
24-OCOCH3 | 172.5 | 172.9 |
|
|
|
24-OCOCH3 | 20.9 | 21.1 |
|
|
|
25-OCOCH3 | 172.1 |
|
|
|
|
25-OCOCH3 | 22.2 |
|
|
|
|
24-OMe |
|
|
| 61.4 |
|
30-OMe |
|
| 51.5 | 51.5 |
|