Position

1a*

(in MeOD)

1b*

(in MeOD)

1c**

(in MeOD)

1d**

(in MeOD)

5a*

(in CDCl3-MeOD)

1

34.6

34.6

34.7

34.6

16.9

2

38.2

38.2

38.2

38.2

32.6

3

219.2

219.3

219.0

219.1

75.7

4

51.1

51.1

51.1

51.1

48.5

5

49.3

49.3

49.4

49.4

37.6

6

21.9

21.9

21.9

21.9

41.8

7

27.9

27.9

28.1

28.1

18.0

8

46.8

46.8

47.0

46.9

52.3

9

21.7

21.7

21.6

21.6

38.2

10

28.5

28.5

28.5

28.6

61.7

11

29.4

29.4

29.4

29.4

39.0

12

34.9

34.9

35.0

35.0

27.7

13

48.5

48.5

48.9

48.9

52.5

14

63.8

63.8

64.4

64.4

41.5

15

32.6

32.6

32.5

32.4

28.7

16

30.4

30.4

30.6

30.5

37.0

17

53.6

53.6

54.1

53.8

31.9

18

18.4

18.5

18.3

18.3

44.1

19

30.6

30.6

30.8

30.8

27.1

20

35.8

35.9

36.6

36.8

141.9

21

18.5

18.6

18.8

18.8

74.9

22

33.0

33.3

34.3

34.5

40.1

23

26.4

26.6

28.7

28.5

11.6

24

77.8

80.7

78.6

90.7

16.1

25

84.2

72.8

73.9

74.4

20.3

26

22.7

25.6

25.8

25.8

18.3

27

22.5

25.9

24.8

25.7

179.3

28

22.6

22.7

22.6

22.6

33.9

29

21.4

21.4

21.4

21.4

117.1

30

180.1

180.1

178.4

178.4

24-OCOCH3

172.5

172.9

24-OCOCH3

20.9

21.1

25-OCOCH3

172.1

25-OCOCH3

22.2

24-OMe

61.4

30-OMe

51.5

51.5